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Beilstein J. Org. Chem. 2015, 11, 504–513, doi:10.3762/bjoc.11.57
Graphical Abstract
Scheme 1: The key experimental results on the DDC 1 reactions with thioketones 2 [19-21].
Figure 1: Diazo compounds 1 and thioketones 2 used in the study.
Scheme 2: General scheme for reactions of DDC 1 with thiobenzophenone (2a).
Figure 2: Optimized structures of the lowest energy Z,E-conformers of diazo compounds 1a–d.
Scheme 3: Reactions of the intermediate thiocarbonyl ylide 7'd via competative 1,5-EC (a) or 1,3-EC (b) follo...